The preparation, crystal structure and magnetic properties of the first tetrameric CoII cluster with a unique planar triangular motif, [Co4L3(H2O)2](ClO4)2·2H2O (1), based on a carboxylic‐functionalized 1,5‐diazacyclooctane (DACO) bridging ligand [1,5‐bis(2‐carboxyethyl)‐DACO], are reported. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004)
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