Highly stable and crystalline mesoporous TiO2 materials have been successfully synthesized by a simple surfactant sulfuric acid carbonization method by using Pluronic triblock copolymers as a template (see figure). The surfactant template is first carbonized by H2SO4 to obtain rigid carbon on the surface of mesochannels that can then support the mesostructure during crystallization at high temperatures.
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Zhang et al. (2010) studied this question.
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