Potassium dithioacetate KCH3CS2 was obtained by action of dithioacetic acid on potassium carbonate in aqueous solution. KCH3CS2 crystallizes orthorhombic within the space group Cmcm. The cell dimensions are: a = 7.689, b = 10.565, and c = 6.490 Å, Z = 4. The coordination number of potassium is 8. Structural refinement by least‐squares method came to a final R = 0.097.
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Borel et al. (1975) studied this question.
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