Three 1 M solutions of CoCl2 at Cl−/Co2+ ratios of 4, 6, and 7 were examined by x-ray diffraction. The Fourier transformed scattering data indicated inner complex formation between Co2+ and Cl− ions for the two solutions more enriched in Cl− ions. Coordination parameters of Co2+ ions were obtained by direct fitting of the structure functions.
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Musinu et al. (1984) studied this question.
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