Anatase TiO2 nanocrystallites have been prepared in 1,4-butanediol, 1,5-pentanediol or 1,6-hexanediol under microwave irradiation by the polyol method. It is demonstrated that the crystallite size less than 10 nm can be controlled by changing the quantity of added water.
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Yamamoto et al. (2002) studied this question.
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