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A procedure for the preparation of benzo[b]thiophene‐3‐carboxaldehyde from 3‐methyl‐benzo[b]thiophene is reported. This aldehyde behaves as a typical reactive aromatic aldehyde with respect to oxidation, reduction, the mixed Cannizzaro reaction, reductive amination and acyloin and other condensation reactions.
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Campaigne et al. (1966) studied this question.
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