A direct process for the trifluoromethylthiolation of allylic and benzylic alcohols under mild conditions has been developed. A wide range of free alcohols underwent nucleophilic substitution in the presence of stable CuSCF3 and BF3 ⋅Et2O to give the corresponding products in good to excellent yields.
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Nikolaienko et al. (2014) studied this question.
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