The title compound 2 is a lithium nitronate which crystallizes out with ethanol. Ethanol crystallizes during the preparation of 2 from 1 and lithium ethoxide outlined below, but is also present as solvent. Remarkable features of crystalline 2 are, in particular, the bonding of Li⊕ to nitronate and ethanol O‐atoms and the OH ⃛O bridges from ethanol to a nitronate O‐atom. equation image
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Klebe et al. (1987) studied this question.
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