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A series of single crystals of tetrakis[3,4,3',4'-bis(ethylenedithio)-2,2',5,5'-tetrathiafulvalene] Re 6 Se 5 Cl 9 .-guest] (2a-d) have been prepared where the monoanion is a hexanuclear chalcohalide rhenium cluster and the neutral guest molecules are dimethylformamide (DMF) in 2a (monoclinic modification) and 2b (triclinic modification), tetrahydrofuran (THF) in 2c, and dioxane in 2d. All four compounds present the same basic structural organization in which conducting organic cation radical slabs are sandwichdn by inorganic cluster monoanion layers
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Pénicaud et al. (1993) studied this question.
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