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The large bulk soft magnetic glassy [(Fe0.5Co0.5)0.75B0.20Si0.05]96Nb4 alloy specimens with the diameters up to 7.7mm have been prepared by water quenching the melt immersed in the molten flux of B2O3. The maximum diameter of the obtained specimens is approximately 1.5 times as large as the previous result for copper mold casting. The bulk specimen with 7.7mm in diameter exhibits the saturation magnetization of 1.13T, the coercivity lower than 20A∕m at room temperature, and the Curie temperature of 732K. This bulk specimen is the thickest of any soft magnetic glassy alloys formed until now.
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Bitoh et al. (2006) studied this question.
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