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Spinel-type Co3O4 nanopyramids grown by CVD starting from Co(hfa)2•TMEDA display attractive features for hydrogen production by photo-reforming of methanol solutions, especially in the presence of oxygen in the reaction medium. To the best of our knowledge, this is the first example of photo-activated H2 generation by means of supported cobalt oxide nanosystems.
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Barreca et al. (2010) studied this question.
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