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The reaction between C60 molecules in a 3-keV electron-irradiated C60 thin film has been studied using in situ Fourier-transform infrared (FTIR) spectroscopy and ex situ laser-desorption FT-mass spectrometry (LD-FTMS). The results of FTIR and LD-FTMS measurements indicate that coalesced C120 species were formed as a main product in the electron-beam (EB)-irradiated film. We studied the kinetics of the reaction by examining the decrease in the amount of C60 molecules as a function of irradiation time and found that the reaction rate exhibits a linear dependence on the reactant concentration and a third-power dependence on the electron dose rate.
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Hara et al. (2000) studied this question.
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