Dimeric Bis(trialkylphosphane)rhodium Chlorides: Preparation and Characterization High‐yield methods for the preparation of (PMe3)3RhCl (2) and [(R3P)2RhCl]2 [R = Me (3a); iPr (3b), and cyclohexyl (3c)] are described. The dimeric nature of 3b in the solid state has been established by an X‐ray analysis.
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Binger et al. (1994) studied this question.
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