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A LC-ES-MS/MS method for the identification of dilignols formed by the oxidative cross-coupling of coniferyl alcohol and apocynol has been developed. The identification is based on the generation of ammonium adduct ions [M + NH 4 ] + by electrospray ionization and thereafter the following fragmentation patterns for the selected precursor ions. Fragmentation of several arylglycerol-β-aryl ether (β-O-4) and phenyl coumarane (β-5) model compounds were studied as a reference.
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Sipilä et al. (2000) studied this question.
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