A mechanochemical synthesis of [Cp*RhCl2]2 has been developed. Under LAG conditions the organometallic complex can be prepared in a shorter reaction time compared to the standard solution-based protocol. The obtained Rh(iii) dimer is then applicable as catalyst in subsequent solvent-free mechanochemical C-H bond functionalisations of 2-phenylpyridine.
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Hernández et al. (2015) studied this question.
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