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The present study reports the application of a gold microelectrode array to determine copper(II) ions by anodic stripping voltammetry (ASV). The microelectrode characterization of the presented working electrode was investigated. Moreover, the way of its preparation ensures its reusability and eco-friendly character, thanks to the use of environmentally benign electrode material. The procedure does not require modification of the surface of the working electrode. Main experimental parameters were optimized, including pH and a concentration of the supporting electrolyte, activation and deposition conditions, and square wave parameters. The calibration graph was linear in the range of Cu(II) concentrations from 2 × 10
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Beckstead et al. (1967) studied this question.
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