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The long-postulated reactive intermediates of polar fluoride-inititated trifluoromethylations with Me(3)SiCF(3) (see scheme) were identified by NMR spectroscopy as [Me(3)Si(CF(3))F](-) and [Me(3)Si(CF(3))(2)](-)(.)
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Maggiarosa et al. (1999) studied this question.
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