A method to recover multi‐gram quantities of limonoid glucosides from citrus molasses using ion‐exchange and styrene/divinylbenzene resins has been developed. A cation exchange resin is used to decolorize the molasses, while an anion exchanger is used to separate limonoid glucosides from other negatively charged compounds. Styrene/divinylbenzene resins are used to bind limonoid glucosides and remove water‐soluble materials. The method affords approximately 5 grams of a water‐soluble powder containing over 60% by weight limonoid glucosides per liter of molasses. An analysis of the efficiency of the method shows that less than 10% of the total limonoid glucosides are lost during recovery.
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Schoch et al. (2002) studied this question.
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