A rare single‐crystal to single crystal (SCSC) transformation assisted by hydrogen bonding was induced thermally. A2D homochiral coordination polymer {[Ni2(L‐tar)2(H2O)2](H2O)3}∞ was irreversibly converted into a 3D homochiral coordination polymer, and the structure was confirmed by X‐ray crystallography and XRD. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2008)
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