The preparation and characterization of functionally terminated polybutadienes by an anionic polymerization technique is described. Prepolymers possessing hydroxyl end‐groups were synthesized via vacuum‐line methods. Characterization was completed through endgroup, functionality, molecular weight, molecular weight distribution, and microstructural analyses. Emphasis was placed on the reproducibility in the properties of the prepolymers, particularly in their functionality.
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Samuel F. Reed (1972) studied this question.
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