We developed an in-situ iodination of organoarsenic homocycles for facile and general As–C bond formation. Quantitative in-situ generations of arsenic diiodides from organoarsenic homocycles and iodine were confirmed by 1H NMR analysis. 9-Phenyl- and 9-methyl-9-arsafluorenes were prepared by this method and their optical properties were studied.
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Kato et al. (2015) studied this question.
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