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Bulk and supported nickel phosphides were successfully synthesized from solid nickel(II)-triphenylphosphine complex by a simple thermal treatment in hydrogen flow at 618 K, and the resulting silica-supported nickel phosphide catalyst exhibited superior activity for sulfur removal from dibenzothiophene over the catalyst prepared from nickel phosphate by conventional temperature-programmed reduction.
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Wang et al. (2009) studied this question.
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