The mass spectra of hydroxymethyltetrathiafulvalenes and bis(hydroxymethyl)tetrathiafulvalenes have been studied by electron ionization, metastable analysis and accurate mass measurements. The elimination of water from molecular ions of bis(hydroxymethyl)tetrathiafulvalenes has been investigated with the aid of isotopic labelling and the structures of the ions thus formed have been established by collision‐induced dissociation studies.
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Blanchard et al. (1994) studied this question.
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