A self‐assembly of carbon nitride (C3N4) and layered double hydroxide (LDH) was constructed by electrostatic interaction. The pristine nitrate‐intercalated Mg‐Al‐LDH is turned to carbonate LDH through anion exchange during the photoreduction of CO2 in aqueous solution. The carbonate anions enriched in the interlayer of LDH exhibit a remarkably high reduction efficiency to CH4 in the presence of a C3N4 photoabsorber and Pd cocatalyst.
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Hong et al. (2014) studied this question.
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