New bis- and trispyrazolylborate (scorpionate) ligands derived from 3-(2,4-dimethoxyphenyl)pyrazole have been synthesized. They can function as N,O-polydentate donors, as was demonstrated in the structure of the octahedral complex Ni[Bp(2,4(OMe)2Ph)]2. The structure of Tl[Tp(2,4(OMe)2Ph)] has also been determined.
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Rheingold et al. (1999) studied this question.
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