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Uniform spherical aggregates of palladium nanoparticles with a mean diameter of 70 nm were produced by stirring of palladium(II) acetate with octa(3-aminopropyl)octasilsesquioxane octahydrochloride ( 1 ) as a cubic-linker in methanol at room temperature via self-organized spherical templates of palladium ions and 1 . Transmission electron microscopy investigation showed that the highly ordered spherical aggregates were composed of the palladium nanoparticles with a size of 4.0 nm.
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Naka et al. (2002) studied this question.
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