The ruthenium-catalyzed oxidation of cyclic acetals with tert-butyl hydroperoxide under mild conditions gives the corresponding glycol monoesters efficiently. The present oxidation reaction provides a useful method for the synthesis of glycol monoesters from 1-alkenes by combination with palladium-catalyzed acetalization of 1-alkenes.
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Murahashi et al. (1992) studied this question.
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