Domain inversion in an (001) section of flux-grown has been produced by applying an electric field to a sample via liquid electrodes. An x-ray anomalous scattering experiment has been used for characterization of the domain reversal. The variation of the diffraction images of inversion domains revealed via anomalous-scattering topography clearly indicates that near-perfect inversion domains have been formed by electric-field poling.
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Hu et al. (1996) studied this question.
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