Effect of Operating Parameters on Oil and Phenolic Extraction Using Supercritical CO2

Supercritical fluid extraction (SFE) with carbon dioxide was used to extract oil from canola press cake. Different operating conditions, e.g. pressure, temperature, and co‐solvent % were investigated to optimize extraction parameters to yield canola meal with <4% oil. The residual oil content in the extracted canola meal reduced to 2.1–2.9% in our experimental trials. Residues of the optimum conditions based on oil yield were compared for the total phenolic content and the main phenolic compounds. Sinapine (the choline ester of sinapic acid) was the major phenolic constituent in both the SFE and n‐hexane extracted canola meals and press cakes. n‐Hexane extracted residues showed the retention of the highest sinapic acid, sinapine, sinapoyl glucose and total phenolic contents (mg/g) while the SF‐extracted residues showed the lowest values for these compounds.