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A concise one‐pot route for the synthesis of 2,3‐dihydroisoxazoles via a dual gold‐iron catalysis has been devised. The method, based on the addition of binucleophilic protected hydroxylamine to propargylic alcohols, enables a one‐pot, highly selective synthesis of these heterocycles (10 examples, up to 86% yield).
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Debleds et al. (2009) studied this question.
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