Crystal structure of [4-t-butyl-2-({[4-(diethylamino)-2-(hydroxy)phenyl]methylidene}amino)phenolato-κ 3 N,N′,O] -(methanol)-(methanolato)-(oxido)-vanadium(V), C 23 H 33 N 2 O 5 V

Q: What does this research mean for the field?

The crystal structure of the vanadium(V) complex C23H33N2O5V is monoclinic, belonging to the P21/c space group with specific unit cell dimensions. Novelty: ClaimNovelty.INCREMENTAL. Consensus alignment: ConsensusAlignment.NEUTRAL.

Yuanlin Li; Yueyue Mao; Chengke Liu; Chenxi Gu; Hongxin Cui; Dai Zeng

doi:10.1515/ncrs-2026-0361

September 4, 2026Zeitschrift für Kristallographie - New Crystal StructuresOpen Access

Crystal structure of [4-t-butyl-2-({[4-(diethylamino)-2-(hydroxy)phenyl]methylidene}amino)phenolato-κ 3 N,N′,O] -(methanol)-(methanolato)-(oxido)-vanadium(V), C 23 H 33 N 2 O 5 V

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Key Points

Determine the single-crystal molecular structure and crystallographic parameters of the vanadium(V) complex C23H33N2O5V.
Performs single-crystal X-ray diffraction data collection at a temperature of 293(2) K.
Solves and refines the crystal structure in the monoclinic space group P21/c.
The compound crystallizes in the monoclinic space group P21/c with unit cell dimensions a = 12.9799(4) Å, b = 18.1601(7) Å, c = 10.3268(3) Å, β = 97.761(3)°, and V = 2411.90(14) Å³ for Z = 4.
Structural refinement yields residual factors of Rgt(F) = 0.0462 and wRref(F2) = 0.1359.

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Implication

Crystallographic analysis reveals the monoclinic structure of a vanadium(V) complex, indicating precise coordination parameters for metal-organic research.

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Li et al. (2026) studied this question.

synapsesocial.com/papers/6a9d1e8328139818eab21734 https://doi.org/10.1515/ncrs-2026-0361

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Crystal structure of [4-t-butyl-2-({[4-(diethylamino)-2-(hydroxy)phenyl]methylidene}amino)phenolato-κ 3 N,N′,O] -(methanol)-(methanolato)-(oxido)-vanadium(V), C 23 H 33 N 2 O 5 V

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Crystal structure of [4-t-butyl-2-({[4-(diethylamino)-2-(hydroxy)phenyl]methylidene}amino)phenolato-κ 3 N,N′,O] -(methanol)-(methanolato)-(oxido)-vanadium(V), C 23 H 33 N 2 O 5 V

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