An unsaturated, highly strained [5]metacyclophane derivative is one description of compound 2, which was obtained by the reaction of the hexahalobispropellane precursor 1 (X C1) with tBuOK in dimethylsulfoxide. Compound 2 was characterized by NMR spectroscopy and high-resolution mass spectrometry.
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Wijsman et al. (1993) studied this question.
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