Enhancement of NMR signals by para-hydrogen induced polarisation allows the rapid characterisation of [IrH2Cl(CO)(PPh3)2] and [IrH2Cl(PPh3)3]: these complexes undergo ligand exchange via a 16-electron complex, [IrH2Cl(PPh3)2], which has a square-based pyramidal structure.
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Sleigh et al. (1996) studied this question.
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