Zinc‐nickel electrodeposits have been widely adopted for surface treatment of automobile body steel sheet for high corrosion resistance. This paper describes the morphology evolution of pulsed electrodeposited zinc‐nickel binary alloys. With an increase in pulse current off‐time, morphologies change from triangular‐pyramidal‐shaped crystals which are hexagonal columnar crystals to pyramidal‐shaped crystals which are hexagonal columnar crystals with two independent c axes and then to pyramidal shaped crystals which are the hexagonal columnar crystals having granular crystals on their (10 · 0)η.
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Kondo et al. (1995) studied this question.
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