The homoleptic, square-planar, d 7 , 15-electron species [NBu 4 ][Ni III (C 6 Cl 5 ) 4 ] 2 is obtained by low-temperature oxidation of [NBu 4 ] 2 [Ni II (C 6 Cl 5 ) 4 ] 1 with Cl 2 .
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Alonso et al. (1997) studied this question.
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