Polycrystalline Mo/MoOx nanoflakes were synthesized via the thermal decomposition of molybdenum carbonyl in the presence of stabilizing surfactants. These nanoflakes were readily transformed into single-crystalline MoO3 and MoS2 nanoparticles within 2 nm diameters by in situ addition of oxygen and sulfur into the colloidal solution.
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Park et al. (2007) studied this question.
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