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The first synthesis of pure tert‐butyl‐substituted (phthalocyaninato)‐ and (2,3‐naphthalocyaninato)ruthenium [(tBu)4‐MacRu] by thermal decomposition of (tBu)4MacRu(L)2 (L = 3‐chloropyridine, ammonia) is described. The compounds were characterized by UV/Vis, IR, and NMR measurements.
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Hanack et al. (1995) studied this question.
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