Small size, monodispersed hexagonal particles of Mg,Al-CO 3 hydrotalcite-like compounds have been synthesized in short periods of time by the microwave−hydrothermal method. An in-depth study of the influence of the irradiation time and the process temperature has been carried out. Well-crystalized materials with relatively high specific surface area values have been prepared in 30 min at 150 °C.
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Benito et al. (2006) studied this question.
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