An aerosol-based synthesis is described that uses N,N-dimethylformamide solutions of boric acid as the aerosol feedstock and NH3 as a nitriding atmosphere for the preparation of hollow spherical morphology BN particles in the size range 1−5 μm. These particles display unusually high surface areas (500−1400 m2/g) and microporosity.
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Wood et al. (2006) studied this question.
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