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A highly symmetrical three-dimensional (3D) water network containing cage-shaped tetradecameric water cluster units (H 2 O) 14 is observed in the crystalline 3D metal−organic framework materials 1 and 2 . This is a rare demonstration of a 3D water clathrate network trapped in a cavity of a 3D metal−organic framework, and there are no classical hydrogen bonding interactions within the skeleton of the metal−organic framework.
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Jin et al. (2010) studied this question.
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