Three-dimensional flower-like In 2 O 3 nanostructures with a uniform diameter of ca. 0.7−1.2 μm were fabricated via the glycerol-mediated solvothermal reaction followed by calcination. The flower-like indium precursor and In 2 O 3 nanostructures were investigated in detail, and the as-formed indium precursor could be transformed to cubic In 2 O 3 maintaining its original flower-like morphology after calcination. The formation mechanism, which included the formation of In(OH) 3 nanoparticles and their aggregation as well as the reaction between In(OH) 3 and glycerol, was proposed. In addition, the room-temperature photoluminescence (PL) spectrum of the In 2 O 3 nanostructure showed peculiar visible emissions.
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Wang et al. (2009) studied this question.
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