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A collisional induced dissociation (CID) study was done on 3,5,5-trinitropentacyclodecane and 5,5-dinitropentacyclodecane-3-carboxylic acid using tandem high-resolution MS/MS. Fragmentation pathways were determined in the El ionization mode. It was found that fragmentation of the C-N bonds–resulting in losses of the NO2groups–takes place before the fragmentation of the C-C bonds.
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Yinon et al. (1986) studied this question.
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