A new microwave-polythiol method has been developed for preparation of tellurium (Te) with various morphologies. 1,2-Ethanedithiol (EDT) was used as both a reducing reagent and a solvent. Reduction of TeO2 by EDT was achieved by microwave-heating at ≤140 °C for 30 min. The morphology of Te could be controlled by changing experimental parameters.
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Zhu et al. (2003) studied this question.
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