Abstract (1) Vinyl chloride and organohalosilanes were shown to react with finely divided metallic sodium in ethyl ether, and trimethyl-, dimethyldi-, triethyl- and dimethylphenyl- vinylsilanes were prepared. Of these, dimethyldi- and dimethylphenyl-vinylsilane are new compounds and their physical constants were given. (2) Infrared spectra of these four organovinylsilanes were obtained and certain characteristic absorption bands were discussed. (3) Trichlorosilane was found to add to these vinylsilanes at the presence of diacetyl peroxide and four new β-trichlorosilylethyl-silanes were prepared and characterized.
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Motonori Kanazashi (1953) studied this question.
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