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Scratching using a scanning probe microscope (SPM) with a diamond-coated tip was performed on Si(100). The groove size increased linearly with the applied force. By adjusting the applied force, we successfully fabricated a groove with a width of 11 nm and a depth of 0.58 nm at 1 µN. The structural properties of the grooves were evaluated using statistical parameters. The standard deviation (STD) of the groove size increased with increasing the applied force. However, the relative STD (RSD), defined as the STD divided by the mean value, was approximately 10% without depending on the applied force. These results imply that the size fluctuation of grooves can be controlled by the applied force of the tip and that it is possible to perform sub-20 nm nanolithography on Si using SPM scratching.
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Ogino et al. (2007) studied this question.
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