Abstract 17β‐Hydroxy‐[1ξ,2ξ‐3H2]4,6‐androstadien‐3‐one was prepared by the selective reduction of 17β‐hydroxy‐1,4,6‐androstatrien‐3‐one in benzene with tritium over 5% palladium on carbon. After purification by thin layer chromatography and high pressure liquid chromatography, the specific activity was at least 37 Ci/mmol, and the radiochemical purity was greater than 96%.
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Taylor et al. (1980) studied this question.
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