Die Trocknung von tert‐Butylhydroperoxid nach einem einfachen, erstmals gefahrlosen Verfahren

A Simple, Non‐hazardous Procedure for the Preparation of Absolute tert‐Butyl Hydroperoxide from 80% Aqueous Solutions The preparation of absolute tert‐butyl hydroperoxide (< 0.01 mol/l H2O) from commercial 80% aqueous solutions is reduced to a simple experimental procedure by the use of 3Å molecular sieves. In contrast to the usual methods, there is no risk of explosion. A simple color test for the determination of the residual water content is described.