Trifluoromethylthiocopper, a versatile reagent for the introduction of the trifluoromethylthio group into organic compounds, has been prepared in a crystalline form. The thiyl radicals, generated in situ from this precursor, cause the cleavage of the 3S bond of di‐ and trisulfides to give unsymmetrical di‐ and trisulfides. Unsymmeirical n‐butyl trifluoromethyl disulfide is formed by the cleaveage of the CS bond of n‐butyl sulfide.
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Munavalli et al. (1992) studied this question.
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