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The E.P.R.‐spectra of zone‐refined V2O5 are interpreted in terms of a defect centre consisting of an unpaired electron interacting with two equivalent vanadium nuclei separated by an oxygen vacancy. This conception leads to the establishment of a defect formula for V2O5, involving V4+ and V3+ ions. A self‐consistent mechanism is proposed for the formation of the low‐temperature form of non‐stoichiometry in V2O5. Principal values of the approximately axially‐symmetric spin‐Hamiltonian are
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Gillis et al. (1966) studied this question.
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