Abstract 2‐Deoxy‐2‐iodopyranosides 3 , and 9 – 12 were synthesized from sulfanyl alkenes using a “one pot” consecutive cyclization–glycosylation process. Compared with the stepwise procedure, the “one pot” process gave significantly improved yields with similar or slightly lower selectivities. The “onepot” procedure was applied to the synthesis of 2,6‐dideoxy‐2‐iodoglycoside 22 , which was successfully deiodinated to afford the 2,6‐dideoxyglycoside 23 . (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2007)
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Rodríguez et al. (2007) studied this question.
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